FCC Errata Table

CSV December 6, 2016 through December 6, 2018 View all Errata for FCC How to use
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Monograph Title Section Source Publication Page Number Errata Post Date Errata Official Date Target Errata Print Publication Target Online Fix Publication Description
CALCIUM BENZOATE ASSAY/Procedure FCC 11th Edition 193 29-Jun-2018 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 7 of Analysis: Change
Result = (rU/rS) × (CS/CU) × (Mr1/Mr2) × N × 100
to:
Result = (rU/rS) × (CS/CU) × (Mr1/M… Read More
BHA ASSAY/Procedure FCC 11th Edition 143 29-Jun-2018 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of System suitability: Change
3-tert-butyl-4-hydroxyanisole and 2-tert-butyl-4-hydroxyanisole
to:
2-tert-butyl-4-hydroxyanisole and 3-tert-butyl-4-hydroxyanisole
APPENDIX VIII: OLEORESINS CURCUMIN CONTENT FCC 11th Edition 1415 29-Jun-2018 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 6 of Procedure: Change
Result = (A × 100)(165 × b × c)
to:
Result = (A × 100)/(165 × b × c)
BENTONITE IMPURITIES/Inorganic Impurities/Lead FCC 10th Edition 132 27-Apr-2018 1-May-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of Acceptance criteria: Change
(NMT 4 mg/kg).
to:
(NMT 40 mg/kg).
THIAMINE MONONITRATE IDENTIFICATION/D. Procedure FCC 10th Edition 1287 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 2 of Analysis: Change
potassium ferrocyanide TS
to:
potassium ferricyanide TS
SODIUM SELENATE ANHYDROUS ASSAY/Procedure FCC 10th Edition 1199 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 3 of Analysis: Change
add 10 mL of a hydroxylamine hydrochloride solution (0.5/mL).
to:
add 10 mL of a 50% (w/v) hydroxylamine hydrochloride solution.
SODIUM HYDROXIDE SOLUTIONS IMPURITIES/Inorganic Impurities/Mercury FCC 10th Edition 1171 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 1 of Sample solution: Change
Transfer 10.0 g of sample into a 100-mL beaker, dissolve in 15 mL of water, add 2 drops of phenolphthalein TS and, while constantly stirring, slowly neutralize with 1:2 hydrochloric acid. Add 1 mL of 1:5 sulfuric acid and 1 mL of a 40 mg/mL solution of… Read More
SODIUM HYALURONATE (FROM MICROBIAL FERMENTATION) SPECIFIC TESTS/Intrinsic Viscosity FCC 10th Edition 1169 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition First equation in Analysis: Change
ηr = [ti (B/ti2)]/[t0 – (B/ti2)]
to:
ηr = [ti – (B/ti2)]/[t0 − (B/t02)]
SODIUM HYALURONATE (FROM MICROBIAL FERMENTATION) ASSAY/Sodium Hyaluronate Content FCC 10th Edition 1169 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 6 of Calculation: Change
CS = CG × {Z × [100/(100 − hS) × (M1/M2)]}
to:
CS = CG × Z × (M1/M2)
AND
Line 10: Delete
hS= percentage of loss on drying
SODIUM FERROCYANIDE CHEMICAL INFORMATION FCC 10th Edition 1164 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 3: Change
CAS: [13601-19-9]
to:
CAS: [14434-22-1]
APPENDIX X: CARBOHYDRATES (STARCHES, SUGARS, AND RELATED SUBSTANCES) SULFUR DIOXIDE DETERMINATION FCC 10th Edition 1537 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 2: Change
(Based on AOAC Method 962.16)
to:
(Based on AOAC Method 990.28)
TEST SOLUTIONS (TS) AND OTHER REAGENTS Methylene Orange TS Third Supplement to FCC 10th Edition Online 29-Dec-2017 1-Jan-2018 FCC 11th Edition FCC 11th Edition All references to methylene orange TS in FCC should be changed to methyl orange TS
RUTIN CHEMICAL INFORMATION FCC 10th Edition 1116 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 3: Change
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4H-chromen-4-one-3-yl 6-O-α-L-rhamnopyranosyl-β-D-glucoside
to:
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl 6-O-(6-deoxy-α-L-mannopyranosyl)-β-D-glucopyranoside trihydrate
INOSITOL IMPURITIES/Inorganic Impurities/Sulfate, Choride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 655 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,
FRUCTOSE IMPURITIES/Inorganic Impurities/Sulfate, Chloride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 538 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,
FERRIC PHOSPHATE IMPURITIES/Inorganic Impurities FCC 10th Edition 515 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 2 of Arsenic, Arsenic Limit Test, Appendix IIIB: Change
[NOTE—Assemble the special distillation apparatus as shown in Figure 13.]
to:
[NOTE—Assemble the special distillation apparatus as shown in Figure 3.]
AND
Lines 3 and 10 of Mercury/… Read More
CHOLINE CHLORIDE ASSAY/Procedure FCC 10th Edition 313 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 4 of Analysis: Change
mercuric acetate
to:
mercuric acetate TS
LACTITOL ASSAY/Procedure FCC 10th Edition 719 30-Dec-2016 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 2 of Acceptance criteria: Change
calculated on the dried basis
to:
calculated on the anhydrous basis
CARNAUBA WAX DESCRIPTION FCC 10th Edition 271 30-Dec-2016 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 4: Change
Copernicia cereferia (Arruda) Mart.
to:
Copernicia prunifera (Mill.) H.E.Moore
AND
Line 5: Change
C. prunifera (Muell.)
to:
Copernicia cerifera (Arruda) Mart.
L-ARGININE MONOHYDROCHLORIDE CHEMICAL INFORMATION FCC 10th Edition 99 30-Dec-2016 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 3: Change
CAS: [1119-34-12]
to:
CAS: [1119-34-2]
SOLUTIONS AND INDICATORS Test Solutions (TS) and Other Reagents FCC 10th Edition 1624 30-Dec-2016 1-Jan-2017 Second Supplement to FCC 10th Edition FCC 11th Edition Add
Acetic Acid (approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH).