Skip to main content

FCC Errata Table - All

CSV View March 21, 2022 through March 27, 2024 All Errata for FCC How to use
Enter the title of the monograph
Monograph Title Section Source Publication Page Number Errata Effective Date Target Errata Print Publication Target Online Fix Publication Description
FOLIC ACID ASSAY/Procedure FCC Online Online 1-Jul-2023 NA Third Supplement to FCC 13th Edition In System suitability/Suitability requirements/Resolution: Change
NLT 3.6 between calcium formyltetrahydrofolate (related compound A) and folic acid, System suitability solution
to:
NLT 3.6 between leucovorin calcium and folic… Read More
APPENDIX V—ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2023 NA Third Supplement to FCC 13th Edition In Phytase Activity: Change
Sample preparation, Procedure 1: Suspend or dissolve and dilute accurately weighed amounts of sample in Acetate buffer so that 2.0 mL of the final dilution (g/mL) will contain between 0.02 and 0.08 phytase… Read More
OLIVE POMACE OIL, REFINED IDENTIFICATION/H. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
CITRIC ACID SPECIFIC TESTS/Oxalate FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Transfer the solution into a glass cylinder with a ground glass stopper and add an equal volume of concentrated hydrochloric acid and 0.25 mL of 5% potassium ferricyanate solution.
to:
Transfer the solution into a glass cylinder… Read More
OLIVE OIL, EXTRA VIRGIN AND VIRGIN IDENTIFICATION/L. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
HYDROXYPROPYL METHYLCELLULOSE ASSAY/Procedure FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Internal standard solution: Change
Dilute 2.5 g of toluene to 1000 mL with o-xylene.
to:
Dilute 2.5 g of toluene to 100 mL with o-xylene.
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition In Invertase Sumner Unit Activity/Analysis/paragraph 4: Change
To prepare the glucose standards, add 1 mL of the Standard sucrose solution to each of the 3 appropriate Sucrose substrate solution test tubes.
to:
To prepare the… Read More
DEXTROSE IMPURITIES/Inorganic Impurities FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition Change
Chloride
Sample: 2.0 g
Acceptance criteria: Sample shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid. (NMT 0.018%)
to:
Chloride, Chloride and Sulfate Limit Test, Chloride… Read More
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Plant Proteolytic Activity: Change
Citric scid solution (0.05 M):
to:
Citric acid solution (0.05 M):
APPENDIX XVI: PROTEIN-BASED INGREDIENTS GUIDANCE STANDARD FOR UHPLC-MS/MS SCREENING OF NITROGEN-CONTAINING ADULTERANTS IN MILK INGREDIENTS FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Table 5a: Change
Isobutlyene diurea
to:
Isobutylidene diurea
APPENDIX XVI: PROTEIN-BASED INGREDIENTS CAPILLARY GEL ELECTROPHORESIS FOR IDENTIFICATION OF FOREIGN PROTEINS IN WHEY PROTEIN INGREDIENTS FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Principle: Change
The threshold of detection is set as a trade-off between these two constrains
to:
The threshold of detection is set as a trade-off between these two constraints
TEST SOLUTIONS (TS) AND OTHER REAGENTS Acetic Acid FCC 12th Edition 1560 1-Jul-2021 NA Third Supplement to FCC 12th Edition Change
Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH; approximately 17.5 N).
to:
(approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (NLT 99.7% of CH3COOH).
APPENDIX XVI: PROTEIN-BASED INGREDIENTS PEPTIDE MAPPING FOR IDENTIFICATION OF SPECIES IN PROTEIN INGREDIENTS Second Supplement to FCC 12th Edition 1934 1-Jul-2021 Third Supplement to FCC 12th Edition Third Supplement to FCC 12th Edition In Table 10: Change
Rice (glutelin)
to:
Pea (vicilin)
AND
In Table 10: Change
Pea (vicilin)
to:
Rice (glutelin)
CALCIUM ASCORBATE IDENTIFICATION/C. Infrared Absorption FCC 12th Edition 185 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Calcium Absorbate RS
to:
USP Calcium Ascorbate RS
DIMETHYLPOLYSILOXANE IDENTIFICATION/Infrared Absorption FCC 12th Edition 390 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Dimethylpolysiloxane RS
to:
USP Polydimethylsiloxane RS
APPENDIX XVI: PROTEIN-BASED INGREDIENTS DETERMINATION OF STARCH AND STARCH DEGRADATION PRODUCTS IN SKIM MILK POWDER AND NONFAT DRY MILK First Supplement to FCC 12th Edition 1795 1-Jan-2021 FCC 13th Edition Second Supplement to FCC 12th Edition In Sample solution: Change
Filter the supernatant through a 0.2-mm hydrophilic membrane.
to:
Filter the supernatant through a 0.2-μm hydrophilic membrane.
SUCRALOSE CHEMICAL INFORMATION FCC 12th Edition 1123 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change:
Formula wt: 397.64
to:
Formula wt: 397.63
ALPHA-DAMASCONE CHEMICAL INFORMATION FCC 12th Edition 344 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-butene-4-one
to:
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-buten-4-one
CALCIUM PHOSPHATE, MONOBASIC IMPURITIES/Inorganic Impurities/Flouride FCC 12th Edition 211 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition In Analysis: Change
Result = 100 × (CS/CB)/W
to:
Result = 100 × (CS - CB)/W
L-SELENOMETHIONINE CHEMICAL INFORMATION FCC 11th Edition 1054 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
CAS: [1464-42-2]
to:
CAS: [3211-76-5]
VITAMIN A SPECIFIC TESTS/Absorbance Ratio FCC 11th Edition 1239 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
[Note—The Absorbance ratio is the ratio of absorbances corrected/observed at 325 nm.]
to:
[Note—The Absorbance ratio is the ratio of absorbances corrected/observed at 325 nm. Only apply to other forms of Vitamin A in the Assay… Read More
CALCIUM CITRATE ASSAY/Procedure FCC 11th Edition 197 1-Jan-2020 FCC 12th Edition FCC 12th Edition In Analysis: Change
Each mL of 0.05 M disodium EDTA is equivalent to 8.300 mg of Ca3(C6H5O7)2.
to:
Each mL of 0.05 M disodium EDTA is equivalent to 8.307 mg of Ca3(C6H… Read More
STANNOUS CHLORIDE CHEMICAL INFORMATION FCC 11th Edition 1138 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
INS: 521
to:
INS: 512
MALIC ACID CHEMICAL INFORMATION FCC 11th Edition 734 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
CAS: [617-48-1]
to:
CAS: [6915-15-7]
TRIETHYL CITRATE CHEMICAL INFORMATION FCC 11th Edition 1217 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
INS: 1519
to:
INS: 1505
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS SAFETY/Qualified Presumption of Safety by the European Food Safety Authority Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 27: Change
http://www.efsa.europa.eu/en/topics/topic/qps.htm.
to:
http://www.efsa.europa.eu.
POTASSIUM PHOSPHATE, DIBASIC SPECIFIC TESTS/Pyrophosphate FCC 11th Edition 981 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Standard stock solution: Change
The resulting solution contains 1000 mg/mL of pyrophosphate anion
to:
The resulting solution contains 1000 µg/mL of pyrophosphate anion
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION/MFC Used as Probiotics Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 12: Change http://www.cast-science.org/publications/index.cfm/probiotics_their_pot….
to:
Read More
β-APO-8'-CAROTENAL ASSAY/Procedure FCC 11th Edition 84 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the variable definition list in Analysis: Change
A = absorbance of Sample solution B
to:
A = absorbance of the Sample solution
APPENDIX V: ENZYME ASSAYS PLANT PROTEOLYTIC ACTIVITY FCC 11th Edition 1389 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Reagents and Solutions/Stock Standard Solution: Change
USP Papain Reference Standard
to:
USP Papain RS
AND
In the third paragraph of Calculation: Change
USP Papain Reference Standard,
to:
USP Papain RS,
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 18: Change
http://www.efsa.europa.eu/en/efsajournalpub/1944.
to:
http://www.efsa.europa.eu.
LACTYLIC ESTERS OF FATTY ACIDS IMPURITIES/Inorganic Impurities FCC 11th Edition 677 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Lead: Change
Appendix IIB
to:
Appendix IIIB
KRILL OIL IDENTIFICATION/Fatty Acid Composition Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the Monounsaturated fatty acids/cis-Palmitoleic acid Row of the Upper Limit Column of Table 1: Change
6.2
to:
8.5
BETAINE IDENTIFICATION/Infrared Absorption, Spectrophotometric Identification Tests, Appendix IIIC FCC 11th Edition 142 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
The spectrum of the sample exhibits absorption bands at approximately the following wavelengths, which correspond in intensity and wavelength to those in the spectrum of the Reference standard (s = strong, m =… Read More
GLYCERIN IDENTIFICATION/B. Procedure FCC 11th Edition 535 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In Row 4 of Column 1 in the temperature program table: Change
100
to:
120
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In MFC Used to Transform Foods/footnote 4: Change
10.1002/mnfr.201100010, http://www.dfg.de/download/pdf/dfg_im_profil/reden_stellungnahmen/2-1… Read More
KRILL OIL CONTENT OF ASTAXANTHIN First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
NLT 85▲1S(FCC 11) µg/g
to:
NLT 50 µg/g
CALCIUM HYDROXIDE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 11th Edition 202 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Control: Change
5 µg Pb (5 mL of Diluted Standard Lead Solution)
to:
2 µg Pb (2 mL of Diluted Standard Lead Solution)
LITHOL RUBINE BK IMPURITIES/Organic Impurities/Uncombined Intermediates and Products of Side Reactions and Subsidiary Coloring Matters FCC 11th Edition 707 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Standard solution: Change
80 μL of Standard stock solution B,
to:
400 μL of Standard stock solution B,
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 18: Change
[cited 5 March 2011]. Available from http://www.efsa.europa.eu/en/efsajournalpub/1944.htm.
to:
[cited 30 August 2018]. Available from… Read More
CINNAMON BARK OIL, CEYLON TYPE CHEMICAL INFORMATION FCC 11th Edition 293 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In FEMA: Change
2290
to:
2291
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS INTRODUCTION TO MICROBIAL FOOD CULTURES FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 2: Change
[cited 5 March 2011]. Available from ftp://ftp.fao.org/docrep/fao/009/a0512e/a0512e00.pdf.
to:
[cited 30 August 2018]. Available from… Read More
KRILL OIL IDENTIFICATION, Fatty Acid Composition First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Myristic acid Row and Lower Limit Column of Table 1: Change
4.5
to:
3.0
AND
In the Palmitic acid:Myristic acid ratio Row and Upper Limit Column of Table 1: Change
2.8
to:
3.6
AND… Read More
BHA ASSAY/Procedure FCC 11th Edition 143 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of System suitability: Change
3-tert-butyl-4-hydroxyanisole and 2-tert-butyl-4-hydroxyanisole
to:
2-tert-butyl-4-hydroxyanisole and 3-tert-butyl-4-hydroxyanisole
CALCIUM BENZOATE ASSAY/Procedure FCC 11th Edition 193 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 7 of Analysis: Change
Result = (rU/rS) × (CS/CU) × (Mr1/Mr2) × N × 100
to:
Result = (rU/rS) × (CS/CU) × (Mr1/MRead More
APPENDIX VIII: OLEORESINS CURCUMIN CONTENT FCC 11th Edition 1415 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 6 of Procedure: Change
Result = (A × 100)(165 × b × c)
to:
Result = (A × 100)/(165 × b × c)
BENTONITE IMPURITIES/Inorganic Impurities/Lead FCC 10th Edition 132 1-May-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of Acceptance criteria: Change
(NMT 4 mg/kg).
to:
(NMT 40 mg/kg).
SODIUM FERROCYANIDE CHEMICAL INFORMATION FCC 10th Edition 1164 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 3: Change
CAS: [13601-19-9]
to:
CAS: [14434-22-1]
SODIUM HYDROXIDE SOLUTIONS IMPURITIES/Inorganic Impurities/Mercury FCC 10th Edition 1171 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 1 of Sample solution: Change
Transfer 10.0 g of sample into a 100-mL beaker, dissolve in 15 mL of water, add 2 drops of phenolphthalein TS and, while constantly stirring, slowly neutralize with 1:2 hydrochloric acid. Add 1 mL of 1:5 sulfuric acid and 1 mL of a 40 mg/mL solution of… Read More
APPENDIX X: CARBOHYDRATES (STARCHES, SUGARS, AND RELATED SUBSTANCES) SULFUR DIOXIDE DETERMINATION FCC 10th Edition 1537 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 2: Change
(Based on AOAC Method 962.16)
to:
(Based on AOAC Method 990.28)