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FCC Errata Table - All

CSV View November 21, 2022 through November 26, 2024 All Errata for FCC How to use
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Monograph Title Section Source Publication Page Number Errata Effective Date Target Errata Print Publication Target Online Fix Publication Description
L-CARNITINE L-TARTRATE ASSAY FCC Online Online 1-Jul-2024 NA First Supplement to FCC 14th Edition In Acceptance criteria: Change
l-Tartaric acid: 30.8%–32.8%, calculated on the anhydrous basis
l-Carnitine: 67.2%–69.2%, calculated on the anhydrous basis
to:
l-Tartaric acid: 30.8%–32.8%, calculated on the dried… Read More
LYCOPENE FROM BLAKESLEA TRISPORA ASSAY FCC Online Online 1-Jan-2024 NA FCC 14th Edition In footnote 2 in Lycopene: Change
Vydac 281TP54,
to:
Vydac 218TP54,
FOLIC ACID ASSAY/Procedure FCC Online Online 1-Jul-2023 NA Third Supplement to FCC 13th Edition In System suitability/Suitability requirements/Resolution: Change
NLT 3.6 between calcium formyltetrahydrofolate (related compound A) and folic acid, System suitability solution
to:
NLT 3.6 between leucovorin calcium and folic… Read More
APPENDIX V—ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2023 NA Third Supplement to FCC 13th Edition In Phytase Activity: Change
Sample preparation, Procedure 1: Suspend or dissolve and dilute accurately weighed amounts of sample in Acetate buffer so that 2.0 mL of the final dilution (g/mL) will contain between 0.02 and 0.08 phytase… Read More
OLIVE POMACE OIL, REFINED IDENTIFICATION/H. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
CITRIC ACID SPECIFIC TESTS/Oxalate FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Transfer the solution into a glass cylinder with a ground glass stopper and add an equal volume of concentrated hydrochloric acid and 0.25 mL of 5% potassium ferricyanate solution.
to:
Transfer the solution into a glass cylinder… Read More
OLIVE OIL, EXTRA VIRGIN AND VIRGIN IDENTIFICATION/L. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
HYDROXYPROPYL METHYLCELLULOSE ASSAY/Procedure FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Internal standard solution: Change
Dilute 2.5 g of toluene to 1000 mL with o-xylene.
to:
Dilute 2.5 g of toluene to 100 mL with o-xylene.
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition In Invertase Sumner Unit Activity/Analysis/paragraph 4: Change
To prepare the glucose standards, add 1 mL of the Standard sucrose solution to each of the 3 appropriate Sucrose substrate solution test tubes.
to:
To prepare the… Read More
DEXTROSE IMPURITIES/Inorganic Impurities FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition Change
Chloride
Sample: 2.0 g
Acceptance criteria: Sample shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid. (NMT 0.018%)
to:
Chloride, Chloride and Sulfate Limit Test, Chloride… Read More
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Plant Proteolytic Activity: Change
Citric scid solution (0.05 M):
to:
Citric acid solution (0.05 M):
APPENDIX XVI: PROTEIN-BASED INGREDIENTS GUIDANCE STANDARD FOR UHPLC-MS/MS SCREENING OF NITROGEN-CONTAINING ADULTERANTS IN MILK INGREDIENTS FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Table 5a: Change
Isobutlyene diurea
to:
Isobutylidene diurea
APPENDIX XVI: PROTEIN-BASED INGREDIENTS CAPILLARY GEL ELECTROPHORESIS FOR IDENTIFICATION OF FOREIGN PROTEINS IN WHEY PROTEIN INGREDIENTS FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Principle: Change
The threshold of detection is set as a trade-off between these two constrains
to:
The threshold of detection is set as a trade-off between these two constraints
TEST SOLUTIONS (TS) AND OTHER REAGENTS Acetic Acid FCC 12th Edition 1560 1-Jul-2021 NA Third Supplement to FCC 12th Edition Change
Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH; approximately 17.5 N).
to:
(approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (NLT 99.7% of CH3COOH).
APPENDIX XVI: PROTEIN-BASED INGREDIENTS PEPTIDE MAPPING FOR IDENTIFICATION OF SPECIES IN PROTEIN INGREDIENTS Second Supplement to FCC 12th Edition 1934 1-Jul-2021 Third Supplement to FCC 12th Edition Third Supplement to FCC 12th Edition In Table 10: Change
Rice (glutelin)
to:
Pea (vicilin)
AND
In Table 10: Change
Pea (vicilin)
to:
Rice (glutelin)
CALCIUM ASCORBATE IDENTIFICATION/C. Infrared Absorption FCC 12th Edition 185 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Calcium Absorbate RS
to:
USP Calcium Ascorbate RS
DIMETHYLPOLYSILOXANE IDENTIFICATION/Infrared Absorption FCC 12th Edition 390 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Dimethylpolysiloxane RS
to:
USP Polydimethylsiloxane RS
APPENDIX XVI: PROTEIN-BASED INGREDIENTS DETERMINATION OF STARCH AND STARCH DEGRADATION PRODUCTS IN SKIM MILK POWDER AND NONFAT DRY MILK First Supplement to FCC 12th Edition 1795 1-Jan-2021 FCC 13th Edition Second Supplement to FCC 12th Edition In Sample solution: Change
Filter the supernatant through a 0.2-mm hydrophilic membrane.
to:
Filter the supernatant through a 0.2-μm hydrophilic membrane.
SUCRALOSE CHEMICAL INFORMATION FCC 12th Edition 1123 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change:
Formula wt: 397.64
to:
Formula wt: 397.63
ALPHA-DAMASCONE CHEMICAL INFORMATION FCC 12th Edition 344 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-butene-4-one
to:
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-buten-4-one
CALCIUM PHOSPHATE, MONOBASIC IMPURITIES/Inorganic Impurities/Flouride FCC 12th Edition 211 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition In Analysis: Change
Result = 100 × (CS/CB)/W
to:
Result = 100 × (CS - CB)/W
L-SELENOMETHIONINE CHEMICAL INFORMATION FCC 11th Edition 1054 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
CAS: [1464-42-2]
to:
CAS: [3211-76-5]
VITAMIN A SPECIFIC TESTS/Absorbance Ratio FCC 11th Edition 1239 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
[Note—The Absorbance ratio is the ratio of absorbances corrected/observed at 325 nm.]
to:
[Note—The Absorbance ratio is the ratio of absorbances corrected/observed at 325 nm. Only apply to other forms of Vitamin A in the Assay… Read More
CALCIUM CITRATE ASSAY/Procedure FCC 11th Edition 197 1-Jan-2020 FCC 12th Edition FCC 12th Edition In Analysis: Change
Each mL of 0.05 M disodium EDTA is equivalent to 8.300 mg of Ca3(C6H5O7)2.
to:
Each mL of 0.05 M disodium EDTA is equivalent to 8.307 mg of Ca3(C6H… Read More
STANNOUS CHLORIDE CHEMICAL INFORMATION FCC 11th Edition 1138 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
INS: 521
to:
INS: 512
MALIC ACID CHEMICAL INFORMATION FCC 11th Edition 734 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
CAS: [617-48-1]
to:
CAS: [6915-15-7]
TRIETHYL CITRATE CHEMICAL INFORMATION FCC 11th Edition 1217 1-Jan-2020 FCC 12th Edition FCC 12th Edition Change
INS: 1519
to:
INS: 1505
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS SAFETY/Qualified Presumption of Safety by the European Food Safety Authority Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 27: Change
http://www.efsa.europa.eu/en/topics/topic/qps.htm.
to:
http://www.efsa.europa.eu.
POTASSIUM PHOSPHATE, DIBASIC SPECIFIC TESTS/Pyrophosphate FCC 11th Edition 981 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Standard stock solution: Change
The resulting solution contains 1000 mg/mL of pyrophosphate anion
to:
The resulting solution contains 1000 µg/mL of pyrophosphate anion
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION/MFC Used as Probiotics Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 12: Change http://www.cast-science.org/publications/index.cfm/probiotics_their_pot….
to:
Read More
β-APO-8'-CAROTENAL ASSAY/Procedure FCC 11th Edition 84 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the variable definition list in Analysis: Change
A = absorbance of Sample solution B
to:
A = absorbance of the Sample solution
APPENDIX V: ENZYME ASSAYS PLANT PROTEOLYTIC ACTIVITY FCC 11th Edition 1389 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Reagents and Solutions/Stock Standard Solution: Change
USP Papain Reference Standard
to:
USP Papain RS
AND
In the third paragraph of Calculation: Change
USP Papain Reference Standard,
to:
USP Papain RS,
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 18: Change
http://www.efsa.europa.eu/en/efsajournalpub/1944.
to:
http://www.efsa.europa.eu.
LACTYLIC ESTERS OF FATTY ACIDS IMPURITIES/Inorganic Impurities FCC 11th Edition 677 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Lead: Change
Appendix IIB
to:
Appendix IIIB
KRILL OIL IDENTIFICATION/Fatty Acid Composition Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the Monounsaturated fatty acids/cis-Palmitoleic acid Row of the Upper Limit Column of Table 1: Change
6.2
to:
8.5
BETAINE IDENTIFICATION/Infrared Absorption, Spectrophotometric Identification Tests, Appendix IIIC FCC 11th Edition 142 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
The spectrum of the sample exhibits absorption bands at approximately the following wavelengths, which correspond in intensity and wavelength to those in the spectrum of the Reference standard (s = strong, m =… Read More
GLYCERIN IDENTIFICATION/B. Procedure FCC 11th Edition 535 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In Row 4 of Column 1 in the temperature program table: Change
100
to:
120
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In MFC Used to Transform Foods/footnote 4: Change
10.1002/mnfr.201100010, http://www.dfg.de/download/pdf/dfg_im_profil/reden_stellungnahmen/2-1… Read More
KRILL OIL CONTENT OF ASTAXANTHIN First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
NLT 85▲1S(FCC 11) µg/g
to:
NLT 50 µg/g
CALCIUM HYDROXIDE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 11th Edition 202 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Control: Change
5 µg Pb (5 mL of Diluted Standard Lead Solution)
to:
2 µg Pb (2 mL of Diluted Standard Lead Solution)
LITHOL RUBINE BK IMPURITIES/Organic Impurities/Uncombined Intermediates and Products of Side Reactions and Subsidiary Coloring Matters FCC 11th Edition 707 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Standard solution: Change
80 μL of Standard stock solution B,
to:
400 μL of Standard stock solution B,
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 18: Change
[cited 5 March 2011]. Available from http://www.efsa.europa.eu/en/efsajournalpub/1944.htm.
to:
[cited 30 August 2018]. Available from… Read More
CINNAMON BARK OIL, CEYLON TYPE CHEMICAL INFORMATION FCC 11th Edition 293 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In FEMA: Change
2290
to:
2291
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS INTRODUCTION TO MICROBIAL FOOD CULTURES FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 2: Change
[cited 5 March 2011]. Available from ftp://ftp.fao.org/docrep/fao/009/a0512e/a0512e00.pdf.
to:
[cited 30 August 2018]. Available from… Read More
KRILL OIL IDENTIFICATION, Fatty Acid Composition First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Myristic acid Row and Lower Limit Column of Table 1: Change
4.5
to:
3.0
AND
In the Palmitic acid:Myristic acid ratio Row and Upper Limit Column of Table 1: Change
2.8
to:
3.6
AND… Read More
BHA ASSAY/Procedure FCC 11th Edition 143 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of System suitability: Change
3-tert-butyl-4-hydroxyanisole and 2-tert-butyl-4-hydroxyanisole
to:
2-tert-butyl-4-hydroxyanisole and 3-tert-butyl-4-hydroxyanisole
CALCIUM BENZOATE ASSAY/Procedure FCC 11th Edition 193 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 7 of Analysis: Change
Result = (rU/rS) × (CS/CU) × (Mr1/Mr2) × N × 100
to:
Result = (rU/rS) × (CS/CU) × (Mr1/MRead More
APPENDIX VIII: OLEORESINS CURCUMIN CONTENT FCC 11th Edition 1415 1-Jul-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 6 of Procedure: Change
Result = (A × 100)(165 × b × c)
to:
Result = (A × 100)/(165 × b × c)
BENTONITE IMPURITIES/Inorganic Impurities/Lead FCC 10th Edition 132 1-May-2018 FCC 12th Edition First Supplement to FCC 11th Edition Line 3 of Acceptance criteria: Change
(NMT 4 mg/kg).
to:
(NMT 40 mg/kg).
SODIUM FERROCYANIDE CHEMICAL INFORMATION FCC 10th Edition 1164 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 3: Change
CAS: [13601-19-9]
to:
CAS: [14434-22-1]