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FCC Errata Table - All

CSV View April 18, 2022 through May 14, 2024 All Errata for FCC How to use
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Monograph Title Section Sort ascending Source Publication Page Number Errata Effective Date Target Errata Print Publication Target Online Fix Publication Description
IRON, CARBONYL IMPURITIES/Inorganic Impurities/Lead FCC 9th Edition 611 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Standard solution: Change
Transfer 5.0 mL of Lead nitrate stock solution
to:
Transfer 2.0 mL of Lead nitrate stock solution
AND
Line 15 of Standard solution: Change
The organic solvent layer contains 2.0 µg of lead/mL,and is the Standard… Read More
L-SERINE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 9th Edition 1061 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Add Acceptance criteria: NMT 5 mg/kg
CALCIUM HYDROXIDE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 11th Edition 202 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Control: Change
5 µg Pb (5 mL of Diluted Standard Lead Solution)
to:
2 µg Pb (2 mL of Diluted Standard Lead Solution)
SODIUM METABISULFITE IMPURITIES/Inorganic Impurities/Iron FCC 8th Edition 1046 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 1 of Control: Change
1.0 mL (10 µg Fe)
to:
0.5 mL (5 µg Fe)
SODIUM CHLORIDE IMPURITIES/Inorganic Impurities/Heavy Metals (as Pb)/Method 1 FCC 9th Edition 1078 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of Sample solution: Change
10 g in 35 mL of water
to:
10 g in 35 mL of water. [NOTE—Prepare enough solution to be used for further analysis. Split the final volume into two equal portions.]
AND
Line 1 of Solution B: Change
Transfer 25 mL of Sample solution… Read More
CALCIUM PHOSPHATE, MONOBASIC IMPURITIES/Inorganic Impurities/Flouride FCC 12th Edition 211 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition In Analysis: Change
Result = 100 × (CS/CB)/W
to:
Result = 100 × (CS - CB)/W
SODIUM CHLORIDE IMPURITIES/Inorganic Impurities/Calcium and Magnesium FCC 8th Edition 1023 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 1 of Buffer solution A: Change
67.5 mg
to:
67.5 g
KELP IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 612 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Control: Change
6.0 µg As (6.0 mL Standard Arsenic Solution).
to:
2.0 µg As (2.0 mL Standard Arsenic Solution).
KELP IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 612 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 2 of Apparatus: Change
Figure 14
to:
Figure 4
DEXTROSE IMPURITIES/Inorganic Impurities/Arsenic FCC 9th Edition 360 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Add
Acceptance criteria: NMT 1 mg/kg
SULFUR IMPURITIES/Inorganic Impurities/Arsenic FCC 9th Edition 1173 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
1 mg/kg
to:
NMT 1 mg/kg
DEXTROSE IMPURITIES/Inorganic Impurities FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition Change
Chloride
Sample: 2.0 g
Acceptance criteria: Sample shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid. (NMT 0.018%)
to:
Chloride, Chloride and Sulfate Limit Test, Chloride… Read More
LACTYLIC ESTERS OF FATTY ACIDS IMPURITIES/Inorganic Impurities FCC 11th Edition 677 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Lead: Change
Appendix IIB
to:
Appendix IIIB
FERRIC PHOSPHATE IMPURITIES/Inorganic Impurities FCC 10th Edition 515 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 2 of Arsenic, Arsenic Limit Test, Appendix IIIB: Change
[NOTE—Assemble the special distillation apparatus as shown in Figure 13.]
to:
[NOTE—Assemble the special distillation apparatus as shown in Figure 3.]
AND
Lines 3 and 10 of Mercury/Analysis… Read More
FERROUS CITRATE IMPURITIES/Inorganic Impurities/Sulfate FCC 8th Edition 450 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1: Change
Sulfate, Chloride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB
to:
Sulfate, Chloride and Sulfate Limit Tests, Sulfate Limit Test, Appendix IIIB
CARRAGEENAN IMPURITIES/Inorganic Impurities/Mercury FCC 8th Edition 219 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 15 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CARRAGEENAN IMPURITIES/Inorganic Impurities/Lead FCC 8th Edition 219 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 8 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CARRAGEENAN IMPURITIES/Inorganic Impurities/Cadmium FCC 8th Edition 219 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 8 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CARMINE IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 215 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 10 of Sample solution: Change
Pour the distillate mixture into a 600-mL beaker add 20 mL of bromine water,
to:
Pour the distillate mixture into a 600-mL beaker, and add 20 mL of bromine TS (bromine water),
DEXTRIN IMPURITIES FCC 9th Edition 358 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Row 4 of Column 1 of table: Change
0.1
to:
1.0
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 18: Change
[cited 5 March 2011]. Available from http://www.efsa.europa.eu/en/efsajournalpub/1944.htm.
to:
[cited 30 August 2018]. Available from… Read More
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 18: Change
http://www.efsa.europa.eu/en/efsajournalpub/1944.
to:
http://www.efsa.europa.eu.
PECTINS IDENTIFICATION/Procedure FCC 8th Edition 851 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 16 of Analysis: Delete
Report the value of U as U × 105
AND
Line 1 of Acceptance criteria: Change
U is greater than 0.5, whereas other gums show essentially no change
to:
The amount of unsaturated product produced, U, is NLT 0.5 x 10−5.… Read More
BROMINATED VEGETABLE OIL IDENTIFICATION/Procedure FCC 8th Edition 134 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 2 of Acceptance criteria: Change
an excess of stronger ammonia water.
to:
an excess of ammonia TS, stronger (stronger ammonia water).
BIFIDOBACTERIUM ANIMALIS SSP. LACTIS BI-07 IDENTIFICATION/Nucleic Acid-Based Identification/Acceptance criteria Third Supplement to FCC 9th Edition Online 14-Sep-2015 FCC 10th Edition FCC 10th Edition Line 1 of Primer set 2: Change
The PCR sample preparation prepared with Primer set 2 gives an amplification product of 492 base pairs with an SNP identified as (underlined in the following 15 base pair sequence): GCGGGCAAGTGCTGG.
to:
The PCR sample… Read More
BIFIDOBACTERIUM ANIMALIS SSP. LACTIS HN019 IDENTIFICATION/Nucleic Acid-Based Identification/Acceptance criteria Third Supplement to FCC 9th Edition Online 14-Sep-2015 FCC 10th Edition FCC 10th Edition Line 1 of Primer set 1: Change
The PCR sample preparation prepared with Primer set 1 gives an amplification product of 351 base pairs with an SNP identified as (underlined in the following 15 base pair sequence): CTTCAGATTTTAGGC. The SNP location is 44 base pairs from… Read More
LACTOBACILLUS ACIDOPHILUS NCFM IDENTIFICATION/Nucleic Acid-Based Identification/Acceptance criteria Third Supplement to FCC 9th Edition Online 14-Sep-2015 FCC 10th Edition FCC 10th Edition Line 1 of Primer set 1: Change
The PCR sample preparation prepared with Primer set 1 gives an amplification product of 365 base pairs with two SNPs. The first SNP is identified as (underlined in the following 15 base pair sequence): GAGTAAATTCCATCA and the location is… Read More
LACTOBACILLUS ACIDOPHILUS NCFM IDENTIFICATION/Nucleic Acid-Based Identification FCC 10th Edition 723 1-Jul-2016 FCC 11th Edition FCC 10th Edition Line 6 of PCR amplification: Change
or for 1 min (for Primer set 2; step 4).
to:
or for 1 min (for Primer set 3; step 4).
OLIVE OIL, EXTRA VIRGIN AND VIRGIN IDENTIFICATION/L. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
DIMETHYLPOLYSILOXANE IDENTIFICATION/Infrared Absorption FCC 12th Edition 390 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Dimethylpolysiloxane RS
to:
USP Polydimethylsiloxane RS
BETAINE IDENTIFICATION/Infrared Absorption, Spectrophotometric Identification Tests, Appendix IIIC FCC 11th Edition 142 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
The spectrum of the sample exhibits absorption bands at approximately the following wavelengths, which correspond in intensity and wavelength to those in the spectrum of the Reference standard (s = strong, m =… Read More
KONJAC FLOUR IDENTIFICATION/Heat-Stable Gel Test FCC 10th Edition 705 1-Jul-2016 FCC 11th Edition FCC 10th Edition Line 1 of Sample mixture: Change
prepared by heating the mixture in a water bath
to:
prepared by heating the mixture in a boiling water bath
AND
Line 4 of Analysis: Change
hold quiescently for 2 h
to:
hold for 2 h
OLIVE POMACE OIL, REFINED IDENTIFICATION/H. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
KRILL OIL IDENTIFICATION/Fatty Acid Composition Second Supplement to FCC 11th Edition Online 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the Monounsaturated fatty acids/cis-Palmitoleic acid Row of the Upper Limit Column of Table 1: Change
6.2
to:
8.5
ALGINATE-KONJAC-XANTHAN POLYSACCHARIDE COMPLEX IDENTIFICATION/D. Viscometric Characterization Second Supplement to FCC 8th Edition 1743 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Standard: Change
USP Alginate-Konjac-Xanthan Polysaccharide Complex RS
to:
USP Alginate-Konjac-Xanthan Polysaccharide Complex for Viscosity Identification RS
THIAMINE MONONITRATE IDENTIFICATION/D. Procedure FCC 10th Edition 1287 1-Jan-2018 FCC 11th Edition FCC 11th Edition Line 2 of Analysis: Change
potassium ferrocyanide TS
to:
potassium ferricyanide TS
CALCIUM ASCORBATE IDENTIFICATION/C. Infrared Absorption FCC 12th Edition 185 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Calcium Absorbate RS
to:
USP Calcium Ascorbate RS
GLYCERIN IDENTIFICATION/B. Procedure FCC 11th Edition 535 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In Row 4 of Column 1 in the temperature program table: Change
100
to:
120
ARABINOGALACTAN IDENTIFICATION/B. Procedure FCC 8th Edition 80 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Acceptance criteria: Change
No precipitate forms.
to:
A precipitate forms.
KRILL OIL IDENTIFICATION, Fatty Acid Composition First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Myristic acid Row and Lower Limit Column of Table 1: Change
4.5
to:
3.0
AND
In the Palmitic acid:Myristic acid ratio Row and Upper Limit Column of Table 1: Change
2.8
to:
3.6
AND… Read More
DECYL ACETATE IDENTIFICATION Second Supplement to FCC 9th Edition 1915 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Change the test name
Infrared Absorption
to:
Infrared Spectra
AND
Line 1 of Acceptance criteria: Change
The spectrum of the sample exhibits maxima at the same wavelengths as those in the spectrum displayed below.
to:
The spectrum of the sample exhibits relative… Read More
APPENDIX XVI: PROTEIN-BASED INGREDIENTS GUIDANCE STANDARD FOR UHPLC-MS/MS SCREENING OF NITROGEN-CONTAINING ADULTERANTS IN MILK INGREDIENTS FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Table 5a: Change
Isobutlyene diurea
to:
Isobutylidene diurea
GENERAL PROVISIONS AND REQUIREMENTS FCC SPECIFICATIONS First Supplement to FCC 9th Edition 1807 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 6 of third paragraph: Change
FCC 8, including any Supplement that is current at the time.
to:
the effective edition of FCC, including any Supplement that is effective at the time.
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jan-2022 NA FCC 13th Edition In Plant Proteolytic Activity: Change
Citric scid solution (0.05 M):
to:
Citric acid solution (0.05 M):
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition In Invertase Sumner Unit Activity/Analysis/paragraph 4: Change
To prepare the glucose standards, add 1 mL of the Standard sucrose solution to each of the 3 appropriate Sucrose substrate solution test tubes.
to:
To prepare the… Read More
APPENDIX V—ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 1-Jul-2023 NA Third Supplement to FCC 13th Edition In Phytase Activity: Change
Sample preparation, Procedure 1: Suspend or dissolve and dilute accurately weighed amounts of sample in Acetate buffer so that 2.0 mL of the final dilution (g/mL) will contain between 0.02 and 0.08 phytase… Read More
APPENDIX XIII: ADULTERANTS AND CONTAMINANTS IN FOOD INGREDIENTS DIETHYLENE GLYCOL AND ETHYLENE GLYCOL IN GLYCERIN FCC 10th Edition 1553 1-Jul-2016 FCC 11th Edition FCC 10th Edition Line 1 of Chromatographic system: Change
Chromatographic system,
to:
Chromatographic system, Appendix IIA
APPENDIX XVI: PROTEIN-BASED INGREDIENTS DETERMINATION OF STARCH AND STARCH DEGRADATION PRODUCTS IN SKIM MILK POWDER AND NONFAT DRY MILK First Supplement to FCC 12th Edition 1795 1-Jan-2021 FCC 13th Edition Second Supplement to FCC 12th Edition In Sample solution: Change
Filter the supernatant through a 0.2-mm hydrophilic membrane.
to:
Filter the supernatant through a 0.2-μm hydrophilic membrane.
KRILL OIL DESCRIPTION Third Supplement to FCC 8th Edition 1841 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 6: Change
acetone
to:
solvent
LABDANUM OIL DESCRIPTION FCC 9th Edition 660 1-Jan-2016 FCC 10th Edition FCC 10th Edition Line 6: Change
Cistus ladaniferus L.
to:
Cistus ladanifer L.