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FCC Errata Table - All

CSV View April 18, 2022 through April 19, 2024 All Errata for FCC How to use
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Monograph Title Section Source Publication Page Number Errata Effective Date Target Errata Print Publication Target Online Fix Publication Sort descending Description
DEXTROSE IMPURITIES/Inorganic Impurities FCC Online Online 1-Jul-2022 NA First Supplement to FCC 13th Edition Change
Chloride
Sample: 2.0 g
Acceptance criteria: Sample shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid. (NMT 0.018%)
to:
Chloride, Chloride and Sulfate Limit Test, Chloride… Read More
CASEIN AND CASEINATE SALTS SPECIFIC TESTS/Lactose FCC 9th Edition 263 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 2 of Standard stock solutions: Change
500-mL
to:
100-mL
DEXTRIN IMPURITIES FCC 9th Edition 358 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Row 4 of Column 1 of table: Change
0.1
to:
1.0
DEXTROSE IMPURITIES/Inorganic Impurities/Arsenic FCC 9th Edition 360 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Add
Acceptance criteria: NMT 1 mg/kg
GLUTARALDEHYDE ASSAY/Procedure FCC 9th Edition 532 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 1 of Sample: Change
300 g
to:
300 mg
KRILL OIL SPECIFIC TESTS/Content of Astaxanthin FCC 9th Edition 654 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 4 of Analysis: Change
percent
to:
amount
SUCROMALT DESCRIPTION FCC 9th Edition 1162 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 11: Change
and 40%–60% higher glucooligosaccharides of 12+ DP.
to:
and NLT 40% higher saccharides of DP 3+ and an average of DP 10.
TBHQ SPECIFIC TESTS/Ultraviolet Absorbance (Polynuclear Hydrocarbons) FCC 9th Edition 1192 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 18 of Sample preparation: Change
0.5% solution of 75 : 25 ethanol and water–ascorbic acid.
to:
25:75 (v/v) ethanol water solution containing 0.5% ascorbic acid.
Color Determination SODIUM SULFATE FCC 9th Edition 1366 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 8: Change
tetrahydroquinone sulfate indicator
to
tetrahydroxyquinone indicator(CAS: 319-89-1)5
AND
Add a footnote
[fn: 5 >95% purity (Catalog Number 099165, Matrix Scientific, Columbia, SC, USA), or equivalent].
Glucoamylase Activity (Amyloglucosidase Activity) CALCULATIONS FCC 9th Edition 1397 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 12: Change
µ/g
to:
U/g
Glucoamylase Activity (Amyloglucosidase Activity) CALCULATIONS FCC 9th Edition 1397 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 12: Change
ε
to:
M
L-ARGININE MONOHYDROCHLORIDE CHEMICAL INFORMATION FCC 10th Edition 99 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 3: Change
CAS: [1119-34-12]
to:
CAS: [1119-34-2]
CARNAUBA WAX DESCRIPTION FCC 10th Edition 271 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 4: Change
Copernicia cereferia (Arruda) Mart.
to:
Copernicia prunifera (Mill.) H.E.Moore
AND
Line 5: Change
C. prunifera (Muell.)
to:
Copernicia cerifera (Arruda) Mart.
LACTITOL ASSAY/Procedure FCC 10th Edition 719 1-Jan-2017 FCC 11th Edition Second Supplement to FCC 10th Edition Line 2 of Acceptance criteria: Change
calculated on the dried basis
to:
calculated on the anhydrous basis
BETAINE IDENTIFICATION/Infrared Absorption, Spectrophotometric Identification Tests, Appendix IIIC FCC 11th Edition 142 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
The spectrum of the sample exhibits absorption bands at approximately the following wavelengths, which correspond in intensity and wavelength to those in the spectrum of the Reference standard (s = strong, m =… Read More
CALCIUM HYDROXIDE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 11th Edition 202 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Control: Change
5 µg Pb (5 mL of Diluted Standard Lead Solution)
to:
2 µg Pb (2 mL of Diluted Standard Lead Solution)
CINNAMON BARK OIL, CEYLON TYPE CHEMICAL INFORMATION FCC 11th Edition 293 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In FEMA: Change
2290
to:
2291
GLYCERIN IDENTIFICATION/B. Procedure FCC 11th Edition 535 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In Row 4 of Column 1 in the temperature program table: Change
100
to:
120
LITHOL RUBINE BK IMPURITIES/Organic Impurities/Uncombined Intermediates and Products of Side Reactions and Subsidiary Coloring Matters FCC 11th Edition 707 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Standard solution: Change
80 μL of Standard stock solution B,
to:
400 μL of Standard stock solution B,
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS INTRODUCTION TO MICROBIAL FOOD CULTURES FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 2: Change
[cited 5 March 2011]. Available from ftp://ftp.fao.org/docrep/fao/009/a0512e/a0512e00.pdf.
to:
[cited 30 August 2018]. Available from… Read More
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In MFC Used to Transform Foods/footnote 4: Change
10.1002/mnfr.201100010, http://www.dfg.de/download/pdf/dfg_im_profil/reden_stellungnahmen/2-1… Read More
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture FCC 11th Edition 1453 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In footnote 18: Change
[cited 5 March 2011]. Available from http://www.efsa.europa.eu/en/efsajournalpub/1944.htm.
to:
[cited 30 August 2018]. Available from… Read More
KRILL OIL IDENTIFICATION, Fatty Acid Composition First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Myristic acid Row and Lower Limit Column of Table 1: Change
4.5
to:
3.0
AND
In the Palmitic acid:Myristic acid ratio Row and Upper Limit Column of Table 1: Change
2.8
to:
3.6
AND… Read More
KRILL OIL CONTENT OF ASTAXANTHIN First Supplement to FCC 11th Edition 1743 1-Jan-2019 FCC 12th Edition Second Supplement to FCC 11th Edition In the Acceptance criteria: Change
NLT 85▲1S(FCC 11) µg/g
to:
NLT 50 µg/g
APPENDIX XVI: PROTEIN-BASED INGREDIENTS DETERMINATION OF STARCH AND STARCH DEGRADATION PRODUCTS IN SKIM MILK POWDER AND NONFAT DRY MILK First Supplement to FCC 12th Edition 1795 1-Jan-2021 FCC 13th Edition Second Supplement to FCC 12th Edition In Sample solution: Change
Filter the supernatant through a 0.2-mm hydrophilic membrane.
to:
Filter the supernatant through a 0.2-μm hydrophilic membrane.
OLIVE OIL, EXTRA VIRGIN AND VIRGIN IDENTIFICATION/L. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
OLIVE POMACE OIL, REFINED IDENTIFICATION/H. Specific Extinction, Ultraviolet Absorption FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
CITRIC ACID SPECIFIC TESTS/Oxalate FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Transfer the solution into a glass cylinder with a ground glass stopper and add an equal volume of concentrated hydrochloric acid and 0.25 mL of 5% potassium ferricyanate solution.
to:
Transfer the solution into a glass cylinder… Read More
HYDROXYPROPYL METHYLCELLULOSE ASSAY/Procedure FCC Online Online 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Internal standard solution: Change
Dilute 2.5 g of toluene to 1000 mL with o-xylene.
to:
Dilute 2.5 g of toluene to 100 mL with o-xylene.
SODIUM CHLORIDE SPECIFIC TESTS/Iron FCC 8th Edition 1023 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 3 of Sample solution: Delete
Add 40 mg of ammonium persulfate crystals and 10 mL of ammonium thiocyanate TS.
ALITAME ASSAY/Procedure FCC 8th Edition 33 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 1 of Mobile phase: Change
Acetonitrile and Solution A (1:4)
to:
Dilute 250 mL of acetonitrile to 1 L with Solution A.
CARMINE IMPURITIES/Inorganic Impurities/Lead FCC 8th Edition 215 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 1 of Control: Change
10 µg Pb (10 mL of Diluted Standard Lead Solution)
to:
2 µg Pb (2 mL of Diluted Standard Lead Solution)
GERANIOL OTHER REQUIREMENTS FCC 8th Edition 482 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 1 of Aldehydes: Change
M-2d, Appendix XI
to:
M-2c, Appendix XI
DIOCTYL SODIUM SULFOSUCCINATE SPECIFIC TESTS/Chromatographic Purity FCC 8th Edition 363 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 13 of Analysis: Change
rs is the dioctyl sodium sulfosuccinate response obtained from the Standard solution.
to:
rs is the docusate sodium related compound B response obtained from the Standard solution.
ISOPULEGOL OTHER REQUIREMENTS FCC 8th Edition 608 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 1: Change
Angular Rotation, Aldehydes, M-2d, Appendix XI
to:
Aldehydes, M-2c, Appendix XI
PECTINS IDENTIFICATION/Procedure FCC 8th Edition 851 1-Jan-2013 FCC 9th Edition Second Supplement to FCC 8th Edition Line 16 of Analysis: Delete
Report the value of U as U × 105
AND
Line 1 of Acceptance criteria: Change
U is greater than 0.5, whereas other gums show essentially no change
to:
The amount of unsaturated product produced, U, is NLT 0.5 x 10−5.… Read More
BUTYL STEARATE OTHER REQUIREMENTS/Saponification Value, Appendix VII FCC 9th Edition 177 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
65–180
to:
165–180
IRON, CARBONYL IMPURITIES/Inorganic Impurities/Lead FCC 9th Edition 611 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Standard solution: Change
Transfer 5.0 mL of Lead nitrate stock solution
to:
Transfer 2.0 mL of Lead nitrate stock solution
AND
Line 15 of Standard solution: Change
The organic solvent layer contains 2.0 µg of lead/mL,and is the Standard… Read More
MALIC ACID SPECIFIC TESTS/Optical (Specific) Rotation, Appendix IIB FCC 9th Edition 728 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
[α]D25 between −0.10° and +0.10°
to:
[α]D25 between −0.10° and +0.10°, on the as-is basis
L-SERINE SPECIFIC TESTS/Optical (Specific) Rotation, Appendix IIB FCC 9th Edition 1061 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 3 of Acceptance criteria: Change
+13°
to:
+13.2°
L-SERINE IMPURITIES/Inorganic Impurities/Lead, Lead Limit Test, Appendix IIIB FCC 9th Edition 1061 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Add Acceptance criteria: NMT 5 mg/kg
SODIUM CHLORIDE SPECIFIC TESTS/Iron FCC 9th Edition 1078 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Control solution: Change
Dissolve 10 mL of Iron Standard Solution
to:
Dissolve 1 mL of Iron Standard Solution
SODIUM SELENATE ANHYDROUS ASSAY/Procedure FCC 9th Edition 1120 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
NMT
to:
NLT
SUCROSE IMPURITIES/Organic Impurities/Invert Sugar FCC 9th Edition 1165 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 5 of Internal standard solution: Add
[NOTE—The change in the density of the solution due to addition of the lactose is insignificant, therefore 200 mL is equivalent to 200 g.]
AND
Line 26 of Analysis: Change
RRF = (HL/HS) × [(WSDF × W… Read More
FLUORIDE LIMIT TEST METHOD II (ION-SELECTIVE ELECTRODE METHOD A) FCC 9th Edition 1350 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 4 of Fluoride Standard: Change
1000 mg
to:
1000 µg
AND
Line 2 of Fluoride Standard Solution: Delete
to a 1000-mL volumetric flask, and dilute with water to volume. Take 1 mL of this solution and transfer
GENERAL PROVISIONS AND REQUIREMENTS FCC SPECIFICATIONS First Supplement to FCC 9th Edition 1807 1-Jan-2015 FCC 10th Edition Second Supplement to FCC 9th Edition Line 6 of third paragraph: Change
FCC 8, including any Supplement that is current at the time.
to:
the effective edition of FCC, including any Supplement that is effective at the time.
CHOLINE CHLORIDE ASSAY/Procedure FCC 10th Edition 313 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 4 of Analysis: Change
mercuric acetate
to:
mercuric acetate TS
FERRIC PHOSPHATE IMPURITIES/Inorganic Impurities FCC 10th Edition 515 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 2 of Arsenic, Arsenic Limit Test, Appendix IIIB: Change
[NOTE—Assemble the special distillation apparatus as shown in Figure 13.]
to:
[NOTE—Assemble the special distillation apparatus as shown in Figure 3.]
AND
Lines 3 and 10 of Mercury/Analysis… Read More
FRUCTOSE IMPURITIES/Inorganic Impurities/Sulfate, Chloride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 538 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,
INOSITOL IMPURITIES/Inorganic Impurities/Sulfate, Choride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 655 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,