FCC Errata Table - All

CSV View April 18, 2022 through April 19, 2024 All Errata for FCC How to use
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Monograph Title Section Source Publication Page Number Errata Post Date Errata Effective Date Target Errata Print Publication Target Online Fix Publication Description
KELP IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 612 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 2 of Apparatus: Change
Figure 14
to:
Figure 4
ALGINATE-KONJAC-XANTHAN POLYSACCHARIDE COMPLEX IDENTIFICATION/D. Viscometric Characterization Second Supplement to FCC 8th Edition 1743 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Standard: Change
USP Alginate-Konjac-Xanthan Polysaccharide Complex RS
to:
USP Alginate-Konjac-Xanthan Polysaccharide Complex for Viscosity Identification RS
ASTAXANTHIN ESTERS FROM HAEMATOCOCCUS PLUVIALIS ASSAY FCC 8th Edition 89 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 1 of Sample solution: Add
[Note—Prepare one Sample solution as follows from each of the three Sample stock solutions.]
AND
Line 2 of Analysis: Change
Sample solution
to:
Sample solutions
AND
Line 12 of Analysis… Read More
MALIC ACID IMPURITIES/Organic Impurities FCC 8th Edition 683 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 2 of Fumaric and Maleic Acids: Delete
[Note—For all reference standards, do not dry before use and keep the containers tightly closed and protected from light. Determine the water content of the USP Fumaric Acid RS titrimetrically before use and make the necessary correction in… Read More
POTASSIUM PHOSPHATE, MONOBASIC ASSAY/Procedure FCC 8th Edition 944 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 10 of Analysis: Change
A = 5 – x
to:
A = |5 – x|
SODIUM CHLORIDE IMPURITIES/Inorganic Impurities/Calcium and Magnesium FCC 8th Edition 1023 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 1 of Buffer solution A: Change
67.5 mg
to:
67.5 g
SODIUM METABISULFITE IMPURITIES/Inorganic Impurities/Iron FCC 8th Edition 1046 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 1 of Control: Change
1.0 mL (10 µg Fe)
to:
0.5 mL (5 µg Fe)
SODIUM PHOSPHATE, DIBASIC SPECIFIC TESTS/Pyrophosphate FCC 8th Edition 1052 27-Dec-2013 1-Jan-2014 FCC 9th Edition FCC 9th Edition Line 2 of Standard stock solution: Change
tetra sodium pyrophosphate
to:
tetrasodium pyrophosphate
AND
Line 19 of Analysis: Change
tetra sodium pyrophosphate
to:
tetrasodium pyrophosphate
CALCIUM PHOSPHATE, MONOBASIC IMPURITIES/Inorganic Impurities/Flouride FCC 12th Edition 211 26-Jun-2020 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition In Analysis: Change
Result = 100 × (CS/CB)/W
to:
Result = 100 × (CS - CB)/W
SUCRALOSE CHEMICAL INFORMATION FCC 12th Edition 1123 26-Jun-2020 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change:
Formula wt: 397.64
to:
Formula wt: 397.63
ALPHA-DAMASCONE CHEMICAL INFORMATION FCC 12th Edition 344 26-Jun-2020 1-Jul-2020 First Supplement to FCC 12th Edition First Supplement to FCC 12th Edition Change
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-butene-4-one
to:
4-(2,6,6-Trimethyl-2-cyclohexenyl)-2-buten-4-one
CASEIN AND CASEINATE SALTS SPECIFIC TESTS/Lactose FCC 9th Edition 263 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 2 of Standard stock solutions: Change
500-mL
to:
100-mL
DEXTRIN IMPURITIES FCC 9th Edition 358 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Row 4 of Column 1 of table: Change
0.1
to:
1.0
DEXTROSE IMPURITIES/Inorganic Impurities/Arsenic FCC 9th Edition 360 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Add
Acceptance criteria: NMT 1 mg/kg
GLUTARALDEHYDE ASSAY/Procedure FCC 9th Edition 532 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 1 of Sample: Change
300 g
to:
300 mg
KRILL OIL SPECIFIC TESTS/Content of Astaxanthin FCC 9th Edition 654 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 4 of Analysis: Change
percent
to:
amount
SUCROMALT DESCRIPTION FCC 9th Edition 1162 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 11: Change
and 40%–60% higher glucooligosaccharides of 12+ DP.
to:
and NLT 40% higher saccharides of DP 3+ and an average of DP 10.
TBHQ SPECIFIC TESTS/Ultraviolet Absorbance (Polynuclear Hydrocarbons) FCC 9th Edition 1192 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 18 of Sample preparation: Change
0.5% solution of 75 : 25 ethanol and water–ascorbic acid.
to:
25:75 (v/v) ethanol water solution containing 0.5% ascorbic acid.
Color Determination SODIUM SULFATE FCC 9th Edition 1366 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 8: Change
tetrahydroquinone sulfate indicator
to
tetrahydroxyquinone indicator(CAS: 319-89-1)5
AND
Add a footnote
[fn: 5 >95% purity (Catalog Number 099165, Matrix Scientific, Columbia, SC, USA), or equivalent].
Glucoamylase Activity (Amyloglucosidase Activity) CALCULATIONS FCC 9th Edition 1397 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 12: Change
µ/g
to:
U/g
Glucoamylase Activity (Amyloglucosidase Activity) CALCULATIONS FCC 9th Edition 1397 27-Jun-2014 1-Jul-2014 First Supplement to FCC 9th Edition First Supplement to FCC 9th Edition Line 12: Change
ε
to:
M
CALCIUM ASCORBATE IDENTIFICATION/C. Infrared Absorption FCC 12th Edition 185 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Calcium Absorbate RS
to:
USP Calcium Ascorbate RS
TEST SOLUTIONS (TS) AND OTHER REAGENTS Acetic Acid FCC 12th Edition 1560 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition Change
Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH; approximately 17.5 N).
to:
(approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (NLT 99.7% of CH3COOH).
DIMETHYLPOLYSILOXANE IDENTIFICATION/Infrared Absorption FCC 12th Edition 390 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Dimethylpolysiloxane RS
to:
USP Polydimethylsiloxane RS
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 31-Dec-2021 1-Jan-2022 NA FCC 13th Edition In Plant Proteolytic Activity: Change
Citric scid solution (0.05 M):
to:
Citric acid solution (0.05 M):
APPENDIX XVI: PROTEIN-BASED INGREDIENTS GUIDANCE STANDARD FOR UHPLC-MS/MS SCREENING OF NITROGEN-CONTAINING ADULTERANTS IN MILK INGREDIENTS FCC Online Online 31-Dec-2021 1-Jan-2022 NA FCC 13th Edition In Table 5a: Change
Isobutlyene diurea
to:
Isobutylidene diurea
APPENDIX XVI: PROTEIN-BASED INGREDIENTS CAPILLARY GEL ELECTROPHORESIS FOR IDENTIFICATION OF FOREIGN PROTEINS IN WHEY PROTEIN INGREDIENTS FCC Online Online 31-Dec-2021 1-Jan-2022 NA FCC 13th Edition In Principle: Change
The threshold of detection is set as a trade-off between these two constrains
to:
The threshold of detection is set as a trade-off between these two constraints
APPENDIX V: ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 24-Jun-2022 1-Jul-2022 NA First Supplement to FCC 13th Edition In Invertase Sumner Unit Activity/Analysis/paragraph 4: Change
To prepare the glucose standards, add 1 mL of the Standard sucrose solution to each of the 3 appropriate Sucrose substrate solution test tubes.
to:
To prepare the… Read More
DEXTROSE IMPURITIES/Inorganic Impurities FCC Online Online 24-Jun-2022 1-Jul-2022 NA First Supplement to FCC 13th Edition Change
• Chloride
Sample: 2.0 g
Acceptance criteria: Sample shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid. (NMT 0.018%)
to:
• Chloride, Chloride and Sulfate Limit Test, Chloride… Read More
OLIVE OIL, EXTRA VIRGIN AND VIRGIN IDENTIFICATION/L. Specific Extinction, Ultraviolet Absorption FCC Online Online 16-Dec-2022 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
OLIVE POMACE OIL, REFINED IDENTIFICATION/H. Specific Extinction, Ultraviolet Absorption FCC Online Online 16-Dec-2022 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Measure the absorbance of the Sample preparation against Solvent A
to:
Measure the absorbance of the Sample preparation against Solution A
CITRIC ACID SPECIFIC TESTS/Oxalate FCC Online Online 16-Dec-2022 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Analysis: Change
Transfer the solution into a glass cylinder with a ground glass stopper and add an equal volume of concentrated hydrochloric acid and 0.25 mL of 5% potassium ferricyanate solution.
to:
Transfer the solution into a glass cylinder… Read More
HYDROXYPROPYL METHYLCELLULOSE ASSAY/Procedure FCC Online Online 16-Dec-2022 1-Jan-2023 NA Second Supplement to FCC 13th Edition In Internal standard solution: Change
Dilute 2.5 g of toluene to 1000 mL with o-xylene.
to:
Dilute 2.5 g of toluene to 100 mL with o-xylene.
FOLIC ACID ASSAY/Procedure FCC Online Online 30-Jun-2023 1-Jul-2023 NA Third Supplement to FCC 13th Edition In System suitability/Suitability requirements/Resolution: Change
NLT 3.6 between calcium formyltetrahydrofolate (related compound A) and folic acid, System suitability solution
to:
NLT 3.6 between leucovorin calcium and folic… Read More
APPENDIX V—ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 30-Jun-2023 1-Jul-2023 NA Third Supplement to FCC 13th Edition In Phytase Activity: Change
Sample preparation, Procedure 1: Suspend or dissolve and dilute accurately weighed amounts of sample in Acetate buffer so that 2.0 mL of the final dilution (g/mL) will contain between 0.02 and 0.08 phytase… Read More
SOLUTIONS AND INDICATORS Test Solutions (TS) and Other Reagents FCC 10th Edition 1624 30-Dec-2016 1-Jan-2017 Second Supplement to FCC 10th Edition FCC 11th Edition Add
Acetic Acid (approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH).
CHOLINE CHLORIDE ASSAY/Procedure FCC 10th Edition 313 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 4 of Analysis: Change
mercuric acetate
to:
mercuric acetate TS
FERRIC PHOSPHATE IMPURITIES/Inorganic Impurities FCC 10th Edition 515 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 2 of Arsenic, Arsenic Limit Test, Appendix IIIB: Change
[NOTE—Assemble the special distillation apparatus as shown in Figure 13.]
to:
[NOTE—Assemble the special distillation apparatus as shown in Figure 3.]
AND
Lines 3 and 10 of Mercury/Analysis… Read More
FRUCTOSE IMPURITIES/Inorganic Impurities/Sulfate, Chloride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 538 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,
INOSITOL IMPURITIES/Inorganic Impurities/Sulfate, Choride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB FCC 10th Edition 655 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 1: Change
Chloride Limit Test,
to:
Sulfate Limit Test,
RUTIN CHEMICAL INFORMATION FCC 10th Edition 1116 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 3: Change
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4H-chromen-4-one-3-yl 6-O-α-L-rhamnopyranosyl-β-D-glucoside
to:
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl 6-O-(6-deoxy-α-L-mannopyranosyl)-β-D-glucopyranoside trihydrate
APPENDIX XVI: PROTEIN-BASED INGREDIENTS PEPTIDE MAPPING FOR IDENTIFICATION OF SPECIES IN PROTEIN INGREDIENTS Second Supplement to FCC 12th Edition 1934 25-Jun-2021 1-Jul-2021 Third Supplement to FCC 12th Edition Third Supplement to FCC 12th Edition In Table 10: Change
Rice (glutelin)
to:
Pea (vicilin)
AND
In Table 10: Change
Pea (vicilin)
to:
Rice (glutelin)