FCC Errata Table - All

CSV View April 18, 2022 through April 20, 2024 All Errata for FCC How to use
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Monograph Title Section Source Publication Page Number Errata Post Date Errata Effective Date Target Errata Print Publication Target Online Fix Publication Description
RUTIN CHEMICAL INFORMATION FCC 10th Edition 1116 30-Jun-2017 1-Jul-2017 Third Supplement to FCC 10th Edition Third Supplement to FCC 10th Edition Line 3: Change
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4H-chromen-4-one-3-yl 6-O-α-L-rhamnopyranosyl-β-D-glucoside
to:
2-(3,4-Dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl 6-O-(6-deoxy-α-L-mannopyranosyl)-β-D-glucopyranoside trihydrate
β-APO-8'-CAROTENAL ASSAY/Procedure FCC 11th Edition 84 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the variable definition list in Analysis: Change
A = absorbance of Sample solution B
to:
A = absorbance of the Sample solution
LACTYLIC ESTERS OF FATTY ACIDS IMPURITIES/Inorganic Impurities FCC 11th Edition 677 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Lead: Change
Appendix IIB
to:
Appendix IIIB
POTASSIUM PHOSPHATE, DIBASIC SPECIFIC TESTS/Pyrophosphate FCC 11th Edition 981 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Standard stock solution: Change
The resulting solution contains 1000 mg/mL of pyrophosphate anion
to:
The resulting solution contains 1000 µg/mL of pyrophosphate anion
APPENDIX V: ENZYME ASSAYS PLANT PROTEOLYTIC ACTIVITY FCC 11th Edition 1389 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In Reagents and Solutions/Stock Standard Solution: Change
USP Papain Reference Standard
to:
USP Papain RS
AND
In the third paragraph of Calculation: Change
USP Papain Reference Standard,
to:
USP Papain RS,
KRILL OIL IDENTIFICATION/Fatty Acid Composition Second Supplement to FCC 11th Edition Online 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In the Monounsaturated fatty acids/cis-Palmitoleic acid Row of the Upper Limit Column of Table 1: Change
6.2
to:
8.5
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS USES OF MICROBIAL FOOD CULTURES IN FOOD PRODUCTION/MFC Used as Probiotics Second Supplement to FCC 11th Edition Online 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 12: Change http://www.cast-science.org/publications/index.cfm/probiotics_their_pot….
to:
… Read More
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS IDENTITY/Yeast Starter Culture Second Supplement to FCC 11th Edition Online 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 18: Change
http://www.efsa.europa.eu/en/efsajournalpub/1944.
to:
http://www.efsa.europa.eu.
APPENDIX XV: MICROBIAL FOOD CULTURES INCLUDING PROBIOTICS SAFETY/Qualified Presumption of Safety by the European Food Safety Authority Second Supplement to FCC 11th Edition Online 28-Jun-2019 1-Jul-2019 FCC 12th Edition Third Supplement to FCC 11th Edition In footnote 27: Change
http://www.efsa.europa.eu/en/topics/topic/qps.htm.
to:
http://www.efsa.europa.eu.
CALCIUM ASCORBATE IDENTIFICATION/C. Infrared Absorption FCC 12th Edition 185 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Calcium Absorbate RS
to:
USP Calcium Ascorbate RS
TEST SOLUTIONS (TS) AND OTHER REAGENTS Acetic Acid FCC 12th Edition 1560 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition Change
Use ACS reagent-grade Acetic Acid, Glacial (99.7% of CH3COOH; approximately 17.5 N).
to:
(approximately 17.5 N) Use ACS reagent-grade Acetic Acid, Glacial (NLT 99.7% of CH3COOH).
APPENDIX XVI: PROTEIN-BASED INGREDIENTS PEPTIDE MAPPING FOR IDENTIFICATION OF SPECIES IN PROTEIN INGREDIENTS Second Supplement to FCC 12th Edition 1934 25-Jun-2021 1-Jul-2021 Third Supplement to FCC 12th Edition Third Supplement to FCC 12th Edition In Table 10: Change
Rice (glutelin)
to:
Pea (vicilin)
AND
In Table 10: Change
Pea (vicilin)
to:
Rice (glutelin)
DIMETHYLPOLYSILOXANE IDENTIFICATION/Infrared Absorption FCC 12th Edition 390 25-Jun-2021 1-Jul-2021 NA Third Supplement to FCC 12th Edition In Reference standard: Change
USP Dimethylpolysiloxane RS
to:
USP Polydimethylsiloxane RS
FOLIC ACID ASSAY/Procedure FCC Online Online 30-Jun-2023 1-Jul-2023 NA Third Supplement to FCC 13th Edition In System suitability/Suitability requirements/Resolution: Change
NLT 3.6 between calcium formyltetrahydrofolate (related compound A) and folic acid, System suitability solution
to:
NLT 3.6 between leucovorin calcium and folic… Read More
APPENDIX V—ENZYME ASSAYS ENZYME PREPARATIONS USED IN FOOD PROCESSING FCC Online Online 30-Jun-2023 1-Jul-2023 NA Third Supplement to FCC 13th Edition In Phytase Activity: Change
Sample preparation, Procedure 1: Suspend or dissolve and dilute accurately weighed amounts of sample in Acetate buffer so that 2.0 mL of the final dilution (g/mL) will contain between 0.02 and 0.08 phytase… Read More
ARABINOGALACTAN IDENTIFICATION/B. Procedure FCC 8th Edition 80 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Acceptance criteria: Change
No precipitate forms.
to:
A precipitate forms.
ASPARTAME IMPURITIES/Organic Impurities/5-Benzyl-3,6-dioxo-2-piperazineacetic Acid FCC 8th Edition 84 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 10 of Analysis: Change
100%
to:
100
BROMINATED VEGETABLE OIL IDENTIFICATION/Procedure FCC 8th Edition 134 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 2 of Acceptance criteria: Change
an excess of stronger ammonia water.
to:
an excess of ammonia TS, stronger (stronger ammonia water).
CARMINE IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 215 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 10 of Sample solution: Change
Pour the distillate mixture into a 600-mL beaker add 20 mL of bromine water,
to:
Pour the distillate mixture into a 600-mL beaker, and add 20 mL of bromine TS (bromine water),
CARRAGEENAN IMPURITIES/Inorganic Impurities/Cadmium FCC 8th Edition 219 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 8 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CARRAGEENAN IMPURITIES/Inorganic Impurities/Lead FCC 8th Edition 219 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 8 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CARRAGEENAN IMPURITIES/Inorganic Impurities/Mercury FCC 8th Edition 219 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 15 of Analysis: Change
Determine the corrected absorbance values by subtracting the Reagent blank absorbance from each of the Standard solutions and from the Sample solution absorbances.
to:
Determine the corrected absorbance value for the Sample… Read More
CITRONELLOL OTHER REQUIREMENTS FCC 8th Edition 266 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Aldehydes: Change
M2-d, Appendix XI
to:
M2-c, Appendix XI
DIOCTYL SODIUM SULFOSUCCINATE SPECIFIC TESTS/Chromatographic Purity/Table 1 FCC 8th Edition 363 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Row 1 of Column 2: Change
Relative Retention Time (min)
to:
Approximate Retention Time (min)
FERROUS CITRATE IMPURITIES/Inorganic Impurities/Sulfate FCC 8th Edition 450 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1: Change
Sulfate, Chloride and Sulfate Limit Tests, Chloride Limit Test, Appendix IIIB
to:
Sulfate, Chloride and Sulfate Limit Tests, Sulfate Limit Test, Appendix IIIB
INVERT SUGAR ASSAY/Invert Sugar FCC 8th Edition 567 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1: Change
Invert Sugar, Total Solids, Appendix X
to:
Invert Sugar Determination, Appendix X
INVERT SUGAR SPECIFIC TESTS/Total Solids FCC 8th Edition 567 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1: Change
Total Solids, Invert Sugar, Appendix X
to:
Total Solids, Appendix X
AND
Line 1 of Analysis: Change
Determine as directed using the table provided.
to:
Determine as directed under Invert Sugar.
KELP IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 612 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Control: Change
6.0 µg As (6.0 mL Standard Arsenic Solution).
to:
2.0 µg As (2.0 mL Standard Arsenic Solution).
KELP IMPURITIES/Inorganic Impurities/Arsenic FCC 8th Edition 612 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 2 of Apparatus: Change
Figure 14
to:
Figure 4
ALGINATE-KONJAC-XANTHAN POLYSACCHARIDE COMPLEX IDENTIFICATION/D. Viscometric Characterization Second Supplement to FCC 8th Edition 1743 28-Jun-2013 1-Jul-2013 FCC 9th Edition Third Supplement to FCC 8th Edition Line 1 of Standard: Change
USP Alginate-Konjac-Xanthan Polysaccharide Complex RS
to:
USP Alginate-Konjac-Xanthan Polysaccharide Complex for Viscosity Identification RS
IDENTIFICATION TESTS PHOSPHATE FCC 9th Edition 1343 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 3: Change
With ammonium molybdate TS, a yellow precipitate, which is soluble in 6 N ammonium hydroxide, is formed.
to:
Acidified solutions of orthophosphates yield a yellow precipitate with ammonium molybdate TS, which is soluble in 6 N ammonium hydroxide.
PANCREATIN ACTIVITY AMYLASE ACTIVITY FCC 9th Edition 1408 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 14 of Procedure: Change
10.0 mL of 1 N iodine VS,
to:
10.0 mL of 0.1 N iodine VS,
TEST SOLUTIONS (TS) AND OTHER REAGENTS NITRIC ACID FCC 9th Edition 1486 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 2: Delete
(69.0%–71.0% of HNO3)
DECYL ACETATE IDENTIFICATION Second Supplement to FCC 9th Edition 1915 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Change the test name
Infrared Absorption
to:
Infrared Spectra
AND
Line 1 of Acceptance criteria: Change
The spectrum of the sample exhibits maxima at the same wavelengths as those in the spectrum displayed below.
to:
The spectrum of the sample exhibits relative… Read More
SODIUM FERROUS CITRATE IMPURITIES/Inorganic Impurities/Sulfate Second Supplement to FCC 9th Edition 1948 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 3 of Acceptance criteria: Change
(NMT 4.8 mg/kg as SO4.)
to:
(NMT 4.8 g/kg as SO4.)
SUCROSE IMPURITIES/Organic Impurities/Invert Sugar Second Supplement to FCC 9th Edition 1950 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of the second Equation of Analysis: Change
Result = (HS/HL) × (RRFS/WS) × [(WL × WISS2)/200] × 104
to:
Result = (HS/HL) × (RRFS/WS) × [(WL × W… Read More
BRILLIANT BLACK PN IMPURITIES/Uncombined Intermediates and Products of Side Reactions FCC 9th Edition 150 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Row 2 of Column 4 of Table 2: Change
134-34-9
to:
6409-21-8
GLUCOSE SYRUP, DRIED ASSAY/Reducing Sugars Assay FCC 9th Edition 528 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 2 of Acceptance criteria: Change
calculated on the dried basis
to:
calculated on the anhydrous basis
GLUCOSE SYRUP, DRIED SPECIFIC TESTS/Total Solids FCC 9th Edition 528 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
NLT 90% when the reducing sugar content is 88% or greater; NLT 93% when the reducing sugar content is between 20.0% and 88.0%
to:
NLT 90% when the reducing sugar content is 88% or greater, calculated on the anhydrous basis; NLT 93% when the… Read More
OX BILE EXTRACT ASSAY/Procedure FCC 9th Edition 879 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 10 of Analysis: Change
Determine the absorbance of each solution in a 1-cm cell at the wavelength of maximum absorbance at about 650 nm.
to:
Determine the absorbance of each solution in a 1-cm cell at 650 nm.
SODIUM CHLORIDE IMPURITIES/Inorganic Impurities/Heavy Metals (as Pb)/Method 1 FCC 9th Edition 1078 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of Sample solution: Change
10 g in 35 mL of water
to:
10 g in 35 mL of water. [NOTE—Prepare enough solution to be used for further analysis. Split the final volume into two equal portions.]
AND
Line 1 of Solution B: Change
Transfer 25 mL of Sample solution… Read More
SULFUR IMPURITIES/Inorganic Impurities/Arsenic FCC 9th Edition 1173 26-Jun-2015 1-Jul-2015 FCC 10th Edition Third Supplement to FCC 9th Edition Line 1 of Acceptance criteria: Change
1 mg/kg
to:
NMT 1 mg/kg